Thermal Decarboxylation of Some Keto-Acid Hydrazones
Thermal Decarboxylation of Some Keto-Acid Hydrazones"
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THE 2,4-dinitrophenylhydrazones of keto-acids are frequently used to identify these metabolic intermediates. The clear statement by Clift and Cook1 regarding the ready thermal
decarboxylation of the 2,4-dinitrophenylhydrazones of oxaloacetic and acetoacetic acids has sometimes been overlooked, particularly in the use of melting points as a means of identification.
Some of our observations bear on the problem.
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